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Some topics for Process Design Practice course are Mass integration, Advanced column design, Physical property prediction, Process risk assessment and Integration of design and control. This lecture includes: Miscellaneous , Process Economics, General Rule of Thumb, Distillation Columns, Equipment Sizing, Heat Exchangers, Reactors and Vessels, Pinch Analysis, Cp Values, Evonik Site Visit
Typology: Slides
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Based on discussions with industrial design engineers
-^
Each major piece of equipment results in approximately$1,000,000 in capital investment (including installation,engineering time, instrumentation etc. etc.)
-^
Thus
for
a
plant
with
a
reactor
and
two
distillation
columns, the typical price will be around $3,000,
-^
Remember, that this is “order of magnitude” estimation
If identified diameter is beyond the curves found in P&T,assume (
for pricing purposes
) that the separation is
performed in NC columns in parallel all with the samespecifications.
-^
The number of columns required should be based onequal distribution of the cross-sectional area
the
diameter:
max
Aspen^
P&T 2
2
2
Aspen
2
2
2
P&T
2
Aspen
2
P&T D^
20ft
,^
D^
5ft^
Intuitive solution NC = 4 columns
A^
(20ft)
400ft
100ft
4
4
A^
(5ft)
25ft
6.25ft
4
4
A^
100ft
NC^
16 columns
A^
6.25ft ^
^
^
^
^
^
^
^
^
^
^
^
Required information is usually the heat transfer area,apart from furnaces and fired heaters, which may beestimated based on the duty.
-^
Overall heat transfer coefficients can be found in P&T(p. 663 in 5
th^ ed.). Assume an average value.
Assume inlet and outlet temperatures for utility stream.Sample calculations given P&T p. 693.
0
log mean
Q^
U^
A^
T
^
^
Q: Provided by AspenU: Found in P&T ∆T: Calculated after assuming temps.
Heaters, coolers and reactors
-^
Aspen will provide supply and target temperatures aswell as enthalpy change for each hot and cold stream
-^
Remember that a hot stream in pinch terminology willactually be TWO streams in Aspen
Supplytemp
Targettemp
∆H
Integration of streams should bedone using the HeatX model
B
1
2 3 4
The
heat
capacity (CP)
of
a
stream
that
does
undergo any phase changes is readily calculated fromthe information provided by Aspen
Ts^
Tt
Q
CP = Q/
T
For mixtures with very different boiling pointsof the constituents the outlet temperatures inexchangers 1 and 2 will be quite different, butit will still give a better approximation than justan average over the entire temperature range.
Liquid @ T
s^
Vapor @ T
t
Q
Liquid @ T
s^
Liquid @ T
b
Q^1
Vapor @ T
b^
Vapor @ T
t
Q^2
Q^3
Can be specifiedin Aspen ashaving an outlet vapor
fraction of0.
Can be specifiedin Aspen ashaving an outlet^ liquid
fraction of0.
Specify outlettemperature at T
t
docsity.com
Distillation columns and flash drums
-^
Due to dynamic implications, distillation columns shouldnot be directly integrated with the utility system
-^
Evaluate
all
columns
together
in
tabular
form
with
duties and temperature levels
-^
If there is a condenser with a temperature higher thana^
reboiler
in
another
column,
then
those
two
are
candidates for integration.
What to bring?•^
Photo ID (drivers license is preferred)
-^
What not to bring?•^
Cameras (including camera phones)
-^
Cell Phone use is only allowed in buildings
-^
Guns, Drugs or Alcohol (I hope this one is obvious)
-^
What to wear?•^
Long Pants
-^
Closed Shoes (no sandals or flip flops)
-^
Shirts with Sleeves (no tank tops)
-^
Safety Glasses
Tentative schedule