Miscellaneous - Process Design Practice - Lecture Slides, Slides of Process Engineering

Some topics for Process Design Practice course are Mass integration, Advanced column design, Physical property prediction, Process risk assessment and Integration of design and control. This lecture includes: Miscellaneous , Process Economics, General Rule of Thumb, Distillation Columns, Equipment Sizing, Heat Exchangers, Reactors and Vessels, Pinch Analysis, Cp Values, Evonik Site Visit

Typology: Slides

2012/2013

Uploaded on 08/21/2013

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Miscellaneous

General Rule of Thumb –^

Based on discussions with industrial design engineers

-^

Each major piece of equipment results in approximately$1,000,000 in capital investment (including installation,engineering time, instrumentation etc. etc.)

-^

Thus

for

a

plant

with

a

reactor

and

two

distillation

columns, the typical price will be around $3,000,

-^

Remember, that this is “order of magnitude” estimation

Process Economics

Distillation Columns (Continued)–^

If identified diameter is beyond the curves found in P&T,assume (

for pricing purposes

) that the separation is

performed in NC columns in parallel all with the samespecifications.

-^

The number of columns required should be based onequal distribution of the cross-sectional area

NOT

the

diameter:

Equipment Sizing 2:

max

Aspen^

P&T 2

2

2

Aspen

2

2

2

P&T

2

Aspen

2

P&T D^

20ft

,^

D^

5ft^

Intuitive solution NC = 4 columns

A^

(20ft)

400ft

100ft

4

4

A^

(5ft)

25ft

6.25ft

4

4

A^

100ft

NC^

16 columns

A^

6.25ft ^

^

^

^

^

^

 

^

^

^

^

  

^

^

 

Heat Exchangers –^

Required information is usually the heat transfer area,apart from furnaces and fired heaters, which may beestimated based on the duty.

-^

Overall heat transfer coefficients can be found in P&T(p. 663 in 5

th^ ed.). Assume an average value.

–^

Assume inlet and outlet temperatures for utility stream.Sample calculations given P&T p. 693.

Equipment Sizing 3:

0

log mean

Q^

U^

A^

T

^

^

 

Q: Provided by AspenU: Found in P&T ∆T: Calculated after assuming temps.

Units to Include–^

Heaters, coolers and reactors

-^

Aspen will provide supply and target temperatures aswell as enthalpy change for each hot and cold stream

-^

Remember that a hot stream in pinch terminology willactually be TWO streams in Aspen

Pinch Analysis 1:

Supplytemp

Targettemp

∆H

Integration of streams should bedone using the HeatX model

B

1

2 3 4

Identifying the CP values (No phase change)–^

The

heat

capacity (CP)

of

a

stream

that

does

NOT

undergo any phase changes is readily calculated fromthe information provided by Aspen

Pinch Analysis 2:

Ts^

Tt

Q

CP = Q/

T

Approximation

Pinch Analysis 4:

For mixtures with very different boiling pointsof the constituents the outlet temperatures inexchangers 1 and 2 will be quite different, butit will still give a better approximation than justan average over the entire temperature range.

Liquid @ T

s^

Vapor @ T

t

Q

Liquid @ T

s^

Liquid @ T

b

Q^1

Vapor @ T

b^

Vapor @ T

t

Q^2

Q^3

Can be specifiedin Aspen ashaving an outlet vapor

fraction of0.

Can be specifiedin Aspen ashaving an outlet^ liquid

fraction of0.

Specify outlettemperature at T

t

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Units NOT to Include –^

Distillation columns and flash drums

-^

Due to dynamic implications, distillation columns shouldnot be directly integrated with the utility system

-^

Evaluate

all

columns

together

in

tabular

form

with

duties and temperature levels

-^

If there is a condenser with a temperature higher thana^

reboiler

in

another

column,

then

those

two

are

candidates for integration.

Pinch Analysis 5:

Evonik Site Visit – March 1 –^

What to bring?•^

Photo ID (drivers license is preferred)

-^

What not to bring?•^

Cameras (including camera phones)

-^

Cell Phone use is only allowed in buildings

-^

Guns, Drugs or Alcohol (I hope this one is obvious)

-^

What to wear?•^

Long Pants

-^

Closed Shoes (no sandals or flip flops)

-^

Shirts with Sleeves (no tank tops)

-^

Safety Glasses

Other Business

Evonik Site Visit – March 1 (Cont’d) –^

Tentative schedule

Other Business