Preparing Solutions and Dilutions Lab, Lecture notes of Chemistry

Dilutions are prepared by adding extra solvent to a solution of known concentration (also called a “stock” solution) to reduce the concentration of solute. The ...

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Preparing Solutions and Dilutions Lab
Objectives:
Two skills that are
essential
to a chemist are preparing solutions of known molarity (M) and
diluting solutions of known molarity (M) to new, less concentrated solutions. As a basis for
understanding this concept, students will learn:
1) To accurately prepare a stock solution of known molarity.
2) To accurately dilute this solution to a new desired molarity.
Materials:
! (2) 100 mL volumetric
flask with caps
! Funnel
! Balance
! NaCl
! Tap water
! 10 mL graduated cylinder
! dropper
! small beaker filled with
water
Pre-Lab
1. Differentiate between the terms solute and solvent.
2. How many grams of AgNO3 are necessary to make 1.0 L of a 6.0 M stock solution?
3. How would you make 1.0 L of a 0.1 M solution of AgNO3 from your 6.0 M stock solution?
Name:
Date:
Per.
Molarity (M) = moles solute
L solution
Percent by Mass of solute = mass of solute x 100
mass of solution
Molarity by Dilution: M1V1 = M2V2
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Preparing Solutions and Dilutions Lab

Objectives : Two skills that are essential to a chemist are preparing solutions of known molarity (M) and diluting solutions of known molarity (M) to new, less concentrated solutions. As a basis for understanding this concept, students will learn:

  1. To accurately prepare a stock solution of known molarity.
  2. To accurately dilute this solution to a new desired molarity. Materials: ! (2) 100 mL volumetric flask with caps ! Funnel ! Balance ! NaCl ! Tap water ! 10 mL graduated cylinder ! dropper ! small beaker filled with water Pre-Lab
  1. Differentiate between the terms solute and solvent.
  2. How many grams of AgNO 3 are necessary to make 1.0 L of a 6.0 M stock solution?
  3. How would you make 1.0 L of a 0.1 M solution of AgNO 3 from your 6.0 M stock solution? Name: Date: Per.

Molarity (M) = moles solute

L solution

Percent by Mass of solute = mass of solute x 100

mass of solution

Molarity by Dilution: M 1 V 1 = M 2 V 2

Part 1: Preparing a 0.5 M NaCl Stock Solution Background Volumetric flasks (see figure) are designed for easy and accurate preparation of solutions of a given volume. The flask is easily swirled to mix the contents if the liquid level is below the neck. The volume measurement at the fill line is very accurate. The flasks can be stoppered for long term storage of solutions. Procedure – work as accurately as possible!

  1. Obtain a 100 mL volumetric flask.
  2. Calculate the mass (grams) of solid NaCl necessary to prepare 100 mL of a 0.50 M NaCl aqueous stock solution. Show your work in the calculations section.
  3. Use the funnel to add the NaCl solute to the dry volumetric flask.
  4. Fill the flask about halfway with tap water. Be sure to rinse any solute stuck in the neck down into the flask. Swirl to dissolve the solute.
  5. Add solvent carefully to the marked line on the neck of the flask. For the most accuracy, the last drops are best done with dropper or squirt bottle.
  6. Invert the flask several times for final mixing.
  7. Bring your solution and calculations to Mrs. Nielsen for approval and a stamp. Calculations:
    1. Calculate the mass (in grams) of solid NaCl necessary to prepare 100 mL of a 0.50 molar aqueous solution of NaCl. (Hint: Find the # of moles of NaCl, then convert to grams)
    2. What is the percent by mass of NaCl in your stock solution? (Hint: use mass of solution = 100.0 g) Analysis
    3. What is the solute in your solution? What is the solvent?
    4. In your own words, describe the steps you took to make your solution.
    5. Why do you not fill the flask with solvent to the line, and then add the solute? fill line A volumetric flask neck of the flask Teacher Stamp