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Information about a soap making laboratory session held at adm biorenewables education laboratory during the summer academy in 2014. The session covered the learning objectives and outcomes of the soap making process, including the definition of saponification, the role of acids and bases, and the use of essential oils. The document also includes safety instructions and procedures for soap production and curing.
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Summer Academy 06/10/ Gabriel Domingues & Matt Schul
Background
Saponification is a process in which a fat molecule is broken down by sodium hydroxide (lye) into four smaller molecules; three of the new molecules are soap and one is glycerol. In simple terms saponification is the name for a chemical reaction between an acid and a base to form a salt. An acid is a molecule or ion that donates protons or hydrogen ions (H +) and/or accepts electrons, and a base is any substance that donates electrons or hydroxide ions (OH - ) and/or that accepts protons.
When you make soap, you mix an oil or fat (which is your acid) with Sodium Hydroxide or Lye (which is your base) to form soap (which is a salt). There are many different types of acids that will react with your base and saponify. Your acid could be olive oil, coconut oil or vegetable oil just to name a few. Each acid has a unique combination of triglycerides (compounds made of three fatty acids attached to a single glycerol molecule) which combines with the base (sodium hydroxide or lye) differently.
Figure 1. General saponification reaction
Summer Academy 06/10/ Gabriel Domingues & Matt Schul
Health and safety information for materials used:
Safety Checklist:
Spill containment and clean up procedures:
Soap Production
Problem Statement:
You may be aware about the use of triglycerides to produce biodiesel. This lab uses triglycerides to produce soap. Soap making relies on an ester and a strong base to perform a saponification reaction. We will create a small bar of soap with the lab procedure discussed later.
Lab Checklist
Summer Academy 06/10/ Gabriel Domingues & Matt Schul
Emergency Contacts
Jacqulyn Baughman Lab Supervisor Cell: (515) 505-
Marjorie Rover Lab Manager Office: (515) 294-2984 Cell: (319) 230-
Ryan Smith BEI Program Coordinator Office: (515) 294-6244 Cell: (515) 203-1640 Home: (719) 660-
Patrick Johnston Assistant Scientist III Office: (515) 509-0027 Cell: (515) 509-0027 Home: (319) 231-
Approved Trainers: Gabriel Domingues Matt Schul