TITLE: Flame Test Lab, Study notes of Chemical Experimentation

4. 5. 6. MATERIALS: -Sodium Chloride solution. -Copper(II) Chloride ...

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Name:_______________________________ Period:________
1 | P a g e
Flame Test Lab
PURPOSE: The purpose of this experiment is to observe the characteristic flame test colors when
burning different metal cations. Students will use this information to identify an unknown.
SAFETY:
1.
2.
3.
4.
5.
6.
MATERIALS:
-Sodium Chloride solution
-Copper(II) Chloride solution
-Lithium Chloride solution
-Potassium Chloride solution
-Strontium Chloride solution
-Barium Chloride solution
-Calcium Chloride solution
-Unknown salt solution
-Bunsen Burner
-Wood splints
-Metal tongs or test tube clamps
PROCEDURE:
1. Open gas valve and then use flint tool to light Bunsen burner.
2. Adjust Bunsen burner until flame is entirely blue.
3. Obtain a wet wood splint.
4. Hold one end of splint with tongs.
5. Hold the chemical end of splint over the Bunsen burner, near tip of blue flame.
6. Observe the color of the flame.
7. WHEN/IF SPLINT BEGINS TO BURN, EXTINGUISH IN BEAKER OF WATER.
8. Record the flame color observed in data table.
9. Repeat steps 3 through 9 with 6 other chemicals and one unknown.
10. Turn gas valve off to extinguish Bunsen burner.
11. Clean up work area and wash hands.
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Flame Test Lab

PURPOSE: The purpose of this experiment is to observe the characteristic flame test colors when

burning different metal cations. Students will use this information to identify an unknown.

SAFETY:

MATERIALS:

  • Sodium Chloride solution
  • Copper(II) Chloride solution
  • Lithium Chloride solution
  • Potassium Chloride solution
  • Strontium Chloride solution
  • Barium Chloride solution
    • Calcium Chloride solution
    • Unknown salt solution
    • Bunsen Burner
    • Wood splints
    • Metal tongs or test tube clamps

PROCEDURE:

  1. Open gas valve and then use flint tool to light Bunsen burner.
  2. Adjust Bunsen burner until flame is entirely blue.
  3. Obtain a wet wood splint.
  4. Hold one end of splint with tongs.
  5. Hold the chemical end of splint over the Bunsen burner, near tip of blue flame.
  6. Observe the color of the flame.
  7. WHEN/IF SPLINT BEGINS TO BURN, EXTINGUISH IN BEAKER OF WATER.
  8. Record the flame color observed in data table.
  9. Repeat steps 3 through 9 with 6 other chemicals and one unknown.
  10. Turn gas valve off to extinguish Bunsen burner.
  11. Clean up work area and wash hands.

DATA TABLE:

METAL COMPOUND COLOR OF FLAME

Copper Chloride CuCl 2 Lithium Chloride LiCl Potassium Chloride KCl Strontium Chloride SrCl 2 Sodium Chloride NaCl Barium Chloride SrCl 2 Calcium Chloride CaCl 2 Unknown

POST LAB QUESTIONS:

  1. Explain why the metal ions emit different colored lights when they are heated in a flame. Use the terms ground state, excited state, and electrons.
  2. What evidence is there from your results that the characteristic color observed for each compound is due to the metal ion in each case as opposed to the chloride ion? In other words, what ion is the control?

Conclusion:

Use your own words to describe what you did in lab today as well as how you determined the identity of your unknown. (4 sentences)Infer how this analytical lab technique used by Forensic Scientists to solve crimes. (2 sentences)Explain two things you learned from this lab. (2 sentences)