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COURSE TITLE : ANALYTICAL INSTRUMENTATION
COURSE CODE : 6212
COURSE CATEGORY : A
PERIODS/WEEK : 5
PERIODS/SEMESTER: 75
CREDITS : 5
TIME SCHEDULE
Module Topics Period 1 Basics of analysis and absorption spectrometers^18 2 Emission Spectrometers 19 3 pH and Chromatography 19 4 Industrial Analzers 19 TOTAL 75
COURSE OUTCOME
Module G.O. On completion of the study of this module the student will be able
1 To understand the basics of analysis
2 To comprehend the working of absorbtion spectrometers
3 To comprehend the working of Infra Red spectrometers
2 1 To understand the working of emission spectrometers
1 To understand pH measurement
2 To understand the working of chromatograph
4 1 To comprehend the working of different industrial analyzers
On completion of the study the student will be able
MODULE I BASICS OF ANALYSIS AND ABSORPTION SPECTROMETERS
1.1.0 To understand the basics of analysis 1.1.1 To explain the various regions of electromagnetic spectrum 1.1.2 To describe the types of spectrum (absorption and emission) 1.1.3 To illustrate the fundamental laws of photometry. 1.1.4 To explain the basic components of photometer
1.2.0 To comprehend the working of absorbtion spectrometers 1.2.1 To differentiate filter photometers and spectrophotometers 1.2.2 To explain the principle, construction and working of single beam filter photometer 1.2.3 To illustrate the principle, construction and working of double beam filter photometer 1.2.4 To explain the principle, construction and working of single beam spectrophotometer 1.2.5 To describe the principle, construction and working of double beam spectrophotometer
1.3.0 To comprehend the working of Infrared spectrophotometer 1.3.1 To describe the basic components of infrared spectrophotometer. 1.3.2 To explain the working of I.R spectrophotometer
MODULE II EMISSION SPECTROMETERS
2.1.0 To understand the working of emission spectrometers 2.1.1 To explain the working of flame photometer 2.1.2 To describe the method of analysis by using flame photometer 2.1.3 To illustrate the principle of mass spectrometer 2.1.4 To explain the construction & working of magnetic deflection mass spectrometer 2.1.5 To explain the construction & working of time of flight mass spectrometer. 2.1.6 To describe the principle, construction & working of N.M.R spectrometer 2.1.7 To State the principle of Raman Effect 2.1.8 To explain the construction & working of Raman spectrophotometer
MODULE III PH AND CHROMATOGRAPHY
3.1.0 To understand pH measurement and control 3.1.1 To define pH and pH scale 3.1.2 To describe the importance of Buffer solution 3.1.3 To explain the construction and working of Hydrogen electrode 3.1.4 To illustrate the construction and working of glass electrode 3.1.5 To List the sources of errors in glass electrode 3.1.6 To explain the methods of error compensation in glass electrode 3.1.7 To describe the construction and working of calomel electrode 3.1.8 To explain the construction and working of combined pH electrode. 3.1.9 To Explain industrial electrode assembly dip and flow type 3.1.10 To describe the working of digital pH meter 3.1.11 To Explain pH control in effluent treatment
3.2.0 To understand Chromatography 3.2.1 To explain the importance of Chromatograph 3.2.2 To describe the Classification of chromatography 3.2.3 To Specify the principle of gas chromatograph 3.2.4 To explain the construction and working of gas chromatograph 3.2.5 To specify the principle of liquid chromatograph 3.2.6 To explain the construction and working of liquid chromatograph 3.2.7 To describe the construction and working of paper chromatograph
REFERENCES:
- Williard, Dean Merrit & Settle , Instrumental methods of analysis- CBS publishers
- R.S.Khandpur , Handbook of Analytical Instruments- TMH
- Chatwal – Anand , Instrumental methods of Chemical Analysis - Himalaya Publishing House
- R K Jain- Mechanical and Industrial Measurements- Khanna Publishers
- B.L.Theraja ,Engineering Physics – S Chand
