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An example of data analysis using sas software and proc mixed procedure. The experiment involves a split-plot design with three temperatures (t1, t2, t3) and three methods. The data is analyzed to determine the effect of temperature and method on the strength of the paper. Sas code, output, and statistical analysis results.
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MIXED^1 The Mixed ProcedureType 3 Analysis of VarianceSum of Source^ DF^ Squares^ Mean^ Square^
Expected^ Mean Square^ Error^ Term method^2 128.388889^ 64.^
Var(Residual) +^4 Var(repmethod)^ MS(repmethod)+^ Q(method,method*temp) temp^3 434.083333^ 144.^
Var(Residual) +^ Q(temp,methodtemp)^ MS(Residual) methodtemp^6 75.166667^ 12.^
Var(Residual) +^ Q(method*temp)^ MS(Residual) rep^2 77.555556^ 38.^
Var(Residual) +^4 Var(repmethod)^ MS(repmethod)+^12 Var(rep) rep*method^4 36.277778^ 9.^
Var(Residual) +^4 Var(rep*method)^ MS(Residual) Residual^18 71.500000^ 3.^
Var(Residual)^. Type 3 Analysis^ of^ VarianceErrorSource DF F^ Value^ Pr^ > F method 4 7.08^ 0.0485temp 18 36.43^ <.0001methodtemp 18 3.15^ 0.0271rep 4 4.28^ 0.1016repmethod 18 2.28^ 0.1003Residual..^.
Analysis of a^ Split-Plot Experiment using PROC^ MIXED
(^3) The Mixed ProcedureDifferences of Least Squares MeansStandard Effect^ method^ temp^ _method^ _temp^ Estimate
Error^ DF^ t^ Value^ Pr^ > |t|^ Adjustment method^1 2 -2.
1.2295^4 -2.30^ 0.0825^ Tukey-Kramer method^1 3 1.
1.2295^4 1.42^ 0.2277^ Tukey-Kramer method^2 3 4.
1.2295^4 3.73^ 0.0203^ Tukey-KramerDifferences of Least Squares^ MeansAdj^ Adj Effect^ method^ temp^ _method^ _temp^ Adj P
Alpha^ Lower^ Upper^ Lower^ Upper method^1 2 0.
method^1 3 0.
method^2 3 0.
0.05^ 1.1698^ 7.9969^ 0.2015^ 8.9651 Tests of Effect^ SlicesNum DenEffect method DF DF^ F^ Value^ Pr >^ F methodtemp 1 3 18 15.50^ <.0001methodtemp 2 3 18 10.21^ 0.0004method*temp 3 3 18 17.03^ <.