Analysis of a Split-Plot Experiment using SAS and PROC MIXED - Prof. Mervyn G. Marasinghe, Study notes of Statistics

An example of data analysis using sas software and proc mixed procedure. The experiment involves a split-plot design with three temperatures (t1, t2, t3) and three methods. The data is analyzed to determine the effect of temperature and method on the strength of the paper. Sas code, output, and statistical analysis results.

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Pre 2010

Uploaded on 09/02/2009

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Example F18
SAS Program
data paper;
do temp=200,225,250,275;
do rep=1 to 3;
do method=1 to 3;
input strength @;
output;
end;
end;
end;
datalines;
30 34 29 28 31 31 31 35 32
35 41 26 32 36 30 37 40 34
37 38 33 40 42 32 41 39 39
36 42 36 41 40 40 40 44 45
;
run;
proc mixed data=paper noclprint noinfo method=type3 cl;;
class rep method temp;
model strength = method temp method*temp/ddfm=satterth;
random rep rep*method;
lsmeans method/diff cl adj=tukey;
lsmeans method*temp/slice=method;
contrast 'Temp:Linear Trend' temp -3 -1 1 3;
contrast 'T1 vs T2 @ M1' temp 1 -1 0 0
method*temp 1 -1 0 0 0 0 0 0 0 0 0 0;
contrast 'T1 vs T3 @ M1' temp 1 0 -1 0
method*temp 1 0 -1 0 0 0 0 0 0 0 0 0;
contrast 'T1 vs T4 @ M1' temp 1 0 0 -1
method*temp 1 0 0 -1 0 0 0 0 0 0 0 0;
title 'Analysis of a Split-Plot Experiment using PROC MIXED';
run;
pf3
pf4
pf5

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Download Analysis of a Split-Plot Experiment using SAS and PROC MIXED - Prof. Mervyn G. Marasinghe and more Study notes Statistics in PDF only on Docsity!

Example^ F18 SAS Programdata^ paper;do^ temp=^200 ,^225 ,^250 ,^275 ; do^ rep=^1 to^^3 ; do method=^1 to^^3 ; input^ strength @;output;end;end;end;datalines;30 34 29 28 31 31 31 35 3235 41 26 32 36 30 37 40 3437 38 33 40 42 32 41 39 3936 42 36 41 40 40 40 44 45; run ; proc^ mixed^ data=paper noclprint^ noinfo^ method=type

cl;;

class^ rep method temp;model^ strength =^ method^ temp methodtemp/ddfm=satterth;random^ rep repmethod;lsmeans^ method/diff^ cl^ adj=tukey;lsmeans^ method*temp/slice=method;contrast^ 'Temp:Linear Trend'^ temp -^3 -^1

contrast^ 'T1 vs T2 @ M1'^ temp^^1 -^1 0 0^ method*temp^^1 -

contrast^ 'T1 vs T3 @ M1'^ temp^^1 0 -^1 0^ method*temp^^1

0 -^1 0 0 0 0 0 0 0 0 0 ;

contrast^ 'T1 vs T4 @ M1'^ temp^^1 0 0 -^1^ method*temp^^1

0 0 -^1 0 0 0 0 0 0 0 0 ;

title^ 'Analysis of a Split-Plot Experiment using PROC MIXED'; run ;

SAS Output^ Analysis of a^ Split-Plot Experiment using PROC

MIXED^1 The Mixed ProcedureType 3 Analysis of VarianceSum of Source^ DF^ Squares^ Mean^ Square^

Expected^ Mean Square^ Error^ Term method^2 128.388889^ 64.^

Var(Residual) +^4 Var(repmethod)^ MS(repmethod)+^ Q(method,method*temp) temp^3 434.083333^ 144.^

Var(Residual) +^ Q(temp,methodtemp)^ MS(Residual) methodtemp^6 75.166667^ 12.^

Var(Residual) +^ Q(method*temp)^ MS(Residual) rep^2 77.555556^ 38.^

Var(Residual) +^4 Var(repmethod)^ MS(repmethod)+^12 Var(rep) rep*method^4 36.277778^ 9.^

Var(Residual) +^4 Var(rep*method)^ MS(Residual) Residual^18 71.500000^ 3.^

Var(Residual)^. Type 3 Analysis^ of^ VarianceErrorSource DF F^ Value^ Pr^ > F method 4 7.08^ 0.0485temp 18 36.43^ <.0001methodtemp 18 3.15^ 0.0271rep 4 4.28^ 0.1016repmethod 18 2.28^ 0.1003Residual..^.

ContrastsNum^ DenLabel DF^ DF^ F^ Value^ Pr^ > F Temp:Linear Trend 1 18 108.87^ <.0001T1 vs T2 @ M1 1 18 9.44^ 0.0066T1 vs T3 @ M1 1 18 35.29^ <.0001T1 vs T4 @ M1 1 18 32.90^ <.0001 Least Squares^ MeansStandardEffect method temp Estimate Error^ DF^ t Value^ Pr >^ |t|^ Alpha^ Lower^

  • method^1 35.6667 1.2574 3. Upper
  • 28.37 <.0001 0.05 32.1340 39.
    • method^2 38.5000 1.2574 3.
    • 30.62 <.0001 0.05 34.9673 42.
      • method^3 33.9167 1.2574 3.
      • 26.97 <.0001 0.05 30.3840 37.
        • method*temp^1 200 29.6667 1.6044 9.
        • 18.49 <.
          • method*temp^1 225 34.6667 1.6044 9.
          • 21.61 <.
            • method*temp^1 250 39.3333 1.6044 9.
            • 24.52 <.
              • method*temp^1 275 39.0000 1.6044 9.
              • 24.31 <.
                • method*temp^2 200 33.3333 1.6044 9.
                • 20.78 <.
                  • method*temp^2 225 39.0000 1.6044 9.
                  • 24.31 <.
                    • methodtemp^2 250 39.6667 1.6044 9. - 24.72 <. - methodtemp^2 275 42.0000 1.6044 9. - 26.18 <. - methodtemp^3 200 30.6667 1.6044 9. - 19.11 <. - methodtemp^3 225 30.0000 1.6044 9. - 18.70 <. - methodtemp^3 250 34.6667 1.6044 9. - 21.61 <. - methodtemp^3 275 40.3333 1.6044 9. - 25.14 <.

Analysis of a^ Split-Plot Experiment using PROC^ MIXED

(^3) The Mixed ProcedureDifferences of Least Squares MeansStandard Effect^ method^ temp^ _method^ _temp^ Estimate

Error^ DF^ t^ Value^ Pr^ > |t|^ Adjustment method^1 2 -2.

1.2295^4 -2.30^ 0.0825^ Tukey-Kramer method^1 3 1.

1.2295^4 1.42^ 0.2277^ Tukey-Kramer method^2 3 4.

1.2295^4 3.73^ 0.0203^ Tukey-KramerDifferences of Least Squares^ MeansAdj^ Adj Effect^ method^ temp^ _method^ _temp^ Adj P

Alpha^ Lower^ Upper^ Lower^ Upper method^1 2 0.

0.05^ -6.2469^ 0.5802^ -7.2151^ 1.

method^1 3 0.

0.05^ -1.6635^ 5.1635^ -2.6318^ 6.

method^2 3 0.

0.05^ 1.1698^ 7.9969^ 0.2015^ 8.9651 Tests of Effect^ SlicesNum DenEffect method DF DF^ F^ Value^ Pr >^ F methodtemp 1 3 18 15.50^ <.0001methodtemp 2 3 18 10.21^ 0.0004method*temp 3 3 18 17.03^ <.