Solid State Nuclear Track Detectors-Advanced Physics-Lab Report, Exercises of Advanced Physics

This is lab report for Advanced Physics Course. It was submitted to Prof. Dhirendra Kapoor at Alliance University. Its main points are: State, Nuclear, Solid, Detector, Track, Etched, Hours, Radiation, Damage, Direction, Dent, Cosmic, Ray

Typology: Exercises

2011/2012

Uploaded on 07/16/2012

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Abstract
The characteristics of Solid State Nuclear Track Detectors (SSNTDs) and their detection mechanism of
heavy nuclear charge particles, such as alpha particles and fission fragments, were studied. The strips of
CR-39 (Columbia Resin-39), irradiated by Am-241 (alpha source) and Cf-252 (spontaneous fission
source) and after being etched in NaOH 6M solution, were analyzed under optical microscope and
diameters of the spots (tracks) left by alpha particles and fission fragments were measured. The
relationship between track diameter and etching time was studied and critical angle of incidence of the
particle on the strip required for the track formation was also determined.
Introduction
A solid-state nuclear track detector or SSNTD (also known as an etched track detector or a dielectric track
detector, DTD) is a section of a solid material (photographic emulsion, crystal, glass or plastic) exposed
to nuclear radiation (neutrons or charged particles, intermittently as well gamma rays), etched, and
inspected microscopically. The pathway of nuclear particles are imprinted quicker than the body
substance, in addition to the range and form of these trails acquiesce knowledge regarding the charge,
mass, direction of motion of the particles as well as the energy. The benefits over other radiation detectors
include the thorough knowledge accessible on distinctive particles, the perseverance of the passageways
permitting measurements to be made over extended periods of time, and the easy, inexpensive and hearty
construction of the detector.
The foundation of SSNTDs is that charged particles break the detector within nanometers down the path
in such a way that the path can be imprinted persistently more rapidly than the unspoiled substance.
Engraving, characteristically for some hours, extends the dent to tapering depths of micrometer
dimensions, which can be seen with a microscope. For a known particle, the span of the pathway shows
the energy of the particle. The charge can be acquired from the carve rate of the pathway in contrast to
that of the main part. If the particles go through the exterior at normal incidence, the depths are circular;
or else the ellipticity and direction of the elliptical pit mouth suggests the direction of incidence.
SSNTDs are frequently used to learn more about cosmic rays, long-standing radioactive elements, radon
concentration in houses, and the age of geological samples.
A substance frequently used in SSNTDs is polyallyl diglycol carbonate (PADC), also known as Tastrak,
CR-39. It is a transparent, colorless, inflexible plastic with the chemical formula C12H18O7. Etching to
expose radiation damage is typically performed using solutions of caustic alkalis such as sodium
hydroxide, regularly at high temperatures for a number of hours.
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Abstract

The characteristics of Solid State Nuclear Track Detectors (SSNTDs) and their detection mechanism of heavy nuclear charge particles, such as alpha particles and fission fragments, were studied. The strips of CR-39 (Columbia Resin-39), irradiated by Am-241 (alpha source) and Cf-252 (spontaneous fission source) and after being etched in NaOH 6M solution, were analyzed under optical microscope and diameters of the spots (tracks) left by alpha particles and fission fragments were measured. The relationship between track diameter and etching time was studied and critical angle of incidence of the particle on the strip required for the track formation was also determined.

Introduction

A solid-state nuclear track detector or SSNTD (also known as an etched track detector or a dielectric track detector, DTD) is a section of a solid material (photographic emulsion, crystal, glass or plastic) exposed to nuclear radiation (neutrons or charged particles, intermittently as well gamma rays), etched, and inspected microscopically. The pathway of nuclear particles are imprinted quicker than the body substance, in addition to the range and form of these trails acquiesce knowledge regarding the charge, mass, direction of motion of the particles as well as the energy. The benefits over other radiation detectors include the thorough knowledge accessible on distinctive particles, the perseverance of the passageways permitting measurements to be made over extended periods of time, and the easy, inexpensive and hearty construction of the detector.

The foundation of SSNTDs is that charged particles break the detector within nanometers down the path in such a way that the path can be imprinted persistently more rapidly than the unspoiled substance. Engraving, characteristically for some hours, extends the dent to tapering depths of micrometer dimensions, which can be seen with a microscope. For a known particle, the span of the pathway shows the energy of the particle. The charge can be acquired from the carve rate of the pathway in contrast to that of the main part. If the particles go through the exterior at normal incidence, the depths are circular; or else the ellipticity and direction of the elliptical pit mouth suggests the direction of incidence.

SSNTDs are frequently used to learn more about cosmic rays, long-standing radioactive elements, radon concentration in houses, and the age of geological samples.

A substance frequently used in SSNTDs is polyallyl diglycol carbonate (PADC), also known as Tastrak, CR-39. It is a transparent, colorless, inflexible plastic with the chemical formula C 12 H 18 O 7. Etching to expose radiation damage is typically performed using solutions of caustic alkalis such as sodium hydroxide, regularly at high temperatures for a number of hours.

Procedure

  1. Following steps were followed:
  2. Firstly. We were provided with irradiated strips which were etched already in NaOH solution.
  3. There were different strips with different etching time.
  4. Then we calibrated the scale on microscope with calibration strip.
  5. We measured diameter of alpha tracks and took ten readings for each strip.
  6. Same procedure is repeated for fission fragments.
  7. Then graph was plotted between etching time for different strips and track diameters.
  8. Then using following formula efficiency was found:

Where,

Vb = bulk etching rate

Vt = track etching rate

Where,

Dff = Diameter of fission fragments

Dα = Diameter of alpha particles

t = Etching time

Then, critical angel was determined as:

For etching time, t = 10.5 hrs

Dff Dα 23 9 24 8 27 8 23 8 22 8 25 7 24 8 23 8 24 7 22 9 Average = 23.7 μm Average = 8 μm

Average Dff = 23.7 μm

Average Dα = 8 μm

Discussion

The spots produce by fission-fragments was having larger diameter than that of alpha-particles. The reason is that fission fragments have a wide spectrum from lighter (A: 60-120) and heavier (A: 120-160) fragments. The lightest fragments produced is even heavier that alpha-particle. That’s the reason that F.F caused more damaged than alpha-particle.

The curve between etching-time and diameter is an increasing curve. The etchant doesn’t get enough time to dissolve the damaged area for smaller etching-time. In case of large etching time the revere is prominent.

This detector cannot be used for neutron and gamma-rays because they are not directly ionizing particles. Beta rays also don’t produce tracks or spots. This method of detection is suitable for particles heavier than proton.

Conclusion

By taking into account the results of the experiment, it can be concluded that this technique can be implemented in prospecting the radon and ultimately uranium. Efficiency is comparatively poor may be because of our inefficiency in noting dimension of different spots of fission fragments and alpha particles.

Since a CR-39 chip cannot be used again therefore the information is permanent and can’t be erased, as compared with TLD’s. This technique gives the accumulated dose in a given interval of time.

References

  1. Knoll, G.F. ; Radiation Detection and Measurement, John Wiley & Sons (1999)
  2. SSNDT notes provided by instructor.